高锝酰氟

高锝酰氟
识别
CAS号 42246-22-0  checkY
性质
化学式 FO3Tc
摩尔质量 164 g·mol−1
外观 浅黄色片状晶体
熔点 18.3 °C[1]
沸点 ~100 °C[1]
若非注明，所有数据均出自标准状态（25 ℃，100 kPa）下。

高锝酰氟是一种无机化合物，化学式为TcO3F，最初由H. Selig和G. Malm在1963年合成。[2]它可由氟气和二氧化锝反应得到，生成的TcO3F挥发出之后有冷阱收集。[1]它可以由高锝酸钾和五氟化铋在氟化氢中反应得到。[3]它可以水解，生成高锝酸和氢氟酸。[1]它和五氟化砷（或五氟化锑）在氟化氢中反应，可以得到TcO2F2AsF6（或TcO2F2SbF6）。[3]

参考文献

  1. ^ 1.0 1.1 1.2 1.3 H. Selig, J.G. Malm. The preparation and properties of pertechnetyl fluoride, TcO3F. Journal of Inorganic and Nuclear Chemistry. 1963-04, 25 (4): 349–351 [2022-06-27]. doi:10.1016/0022-1902(63)80183-9. （原始内容存档于2022-03-19） （英语）. 
  2. ^ Hubert Schmidbaur, W. H. Eugen Schwarz. Permanganyl Fluoride: A Brief History of the Molecule MnO3F and of Those Who Cared For It. Chemistry – A European Journal. 2021-04-21, 27 (23): 6848–6859 [2022-06-27]. ISSN 0947-6539. PMC 8247864 可免费查阅. PMID 33219726. doi:10.1002/chem.202004759 （英语）. 
  3. ^ 3.0 3.1 Joanna Supeł, Ulrich Abram, Adelheid Hagenbach, Konrad Seppelt. Technetium Fluoride Trioxide, TcO 3 F, Preparation and Properties. Inorganic Chemistry. 2007-07-01, 46 (14): 5591–5595 [2022-06-27]. ISSN 0020-1669. doi:10.1021/ic070333y. （原始内容存档于2022-06-30） （英语）. 

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