高氯酸钬

高氯酸钬

识别
CAS号 14017-54-0(无水)  checkY
14692-19-4(八水)  checkY
14692-16-1(九水)  checkY
性质
化学式 Cl3HoO12
摩尔质量 463.28 g·mol−1
若非注明,所有数据均出自标准状态(25 ℃,100 kPa)下。

高氯酸钬是一种无机化合物,化学式为Ho(ClO4)3,它的水溶液存在[Ho(H2O)8]3+[1]

制备及反应

高氯酸钬可由氧化钬和6 mol/L高氯酸溶液反应制得。[1]它的水合物和六氧化二氯反应,可以得到无水物。[2]

它和硝酸银、2,2'-联苯二甲酸(H2BPDC)、异烟酸(HIN)在水中(NaOH调节pH)进行水热反应,可以得到粉色的[Ho2Ag(IN)2(BPDC)2(H2O)2]·(NO3)·2H2O晶体。[3]

参考文献

  1. ^ 1.0 1.1 Wolfram Rudolph, Gert Irmer. On the Hydration of Heavy Rare Earth Ions: Ho3+, Er3+, Tm3+, Yb3+ and Lu3+—A Raman Study. Molecules. 2019-05-21, 24 (10): 1953 [2023-03-15]. ISSN 1420-3049. PMC 6572539可免费查阅. PMID 31117271. doi:10.3390/molecules24101953. (原始内容存档于2023-03-15) (英语). 
  2. ^ J.L. Pascal, F. Favier, F. Cunin, A. Fitch, G. Vaughan. Crystalline and Molecular Structures of Anhydrous Lanthanide PerchloratesLn(ClO4)3withLn=La, Ce, Pr, Sm, Eu, Ho, Er, Tm, and Lu. Journal of Solid State Chemistry. 1998-09, 139 (2): 259–265 [2023-03-15]. doi:10.1006/jssc.1998.7838. (原始内容存档于2018-06-05) (英语). 
  3. ^ Xiao-Ming Lin, Yu-Jia Ding, Shui-Mei Liang, Si-Xiao Ge, Lei-Ming Wei, Ji-Qing Xie, Gang Zhang, Yue-Peng Cai. Two series of Ln( iii )–Ag( i ) heterometallic–organic frameworks constructed from isonicotinate and 2,2′-biphenyldicarboxylate: synthesis, structure and photoluminescence properties. CrystEngComm. 2015, 17 (20): 3800–3808 [2023-03-15]. ISSN 1466-8033. doi:10.1039/C5CE00478K (英语). 

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